High resolution Scanning Electron Microscope FEI Verios 460L
Ondřej Man
The Verios 460L is an unconventional SEM. Through clever design, the Verios 460L allows for ultra-high resolution imaging at low energy on insulating samples with no conductive coating. The Verios 460L is equipped with a wide array of low and high energy electron detectors including a transmission detector and an energy dispersive X-ray spectrometer.
Electron column/optics specifications
Electron column type | Elstar UC |
---|
Electron source type | Schottky FEG with monochromator |
---|
Imaging modes | field free |
---|
XHR immersion |
EDS optimized |
Beam deceleration (stage bias – 20 V to – 4 kV |
Probe current | 0.8 to 100 nA |
---|
Landing energy | 20 eV to 30 keV |
---|
Detectors available
Imaging detectors | Analytical detectors | Others |
---|
in-lens SE detector (TLD-SE) | energy dispersive spectrometer (EDS) | IR camera for viewing sample/column |
in-lens BSE detector (TLD-BSE) | wavelength dispersive spectrometer (WDS) | Chamber mounted Nav-Cam+ |
in-column SE detector (ICD) | electron backscatter diffraction detector (EBSD) | Integrated beam current measurement |
in-column BSE detector (MD) |
|
|
Everhart-Thornley SE detector (ETD) |
forward-scattered electrons detector (FSD) |
Retractable low voltage, solid-state backscatter electron detector (DBS) |
Retractable STEM detector with BF/DF/HAADF segments |
Resolution
Top resolution | Conditions |
---|
0.6 nm | 30 kV (STEM) |
0.6 nm | 15 – 2 kV |
0.7 nm | 1 kV |
1.0 nm | 500 V (ICD) |
Sample stage
Stage type | Ultra high precision 5-axes piezo-motorized stage |
---|
Axis | Maximum movement [mm] |
---|
X, Y | 100 |
Z | 20 |
tilt | – 10 ° to + 60 ° |
rotation | 720 ° stroke |
Positioning accuracy/repeatability |
---|
X, Y repeatability 0.5 μm |
X, Y accuracy < 1.5 μm (85 % tolerance interval) |
Mechanically tilt eucentric stage with < 5 μm image motion when tilting 0 ° to 52 ° |
Maximum sample sizes
Maximum size | 100 mm diameter with full rotation |
Maximum sample thickness (via loadlock) | 15 mm incl. holder |
Maximum sample thickness (via chamber door) | 27.8 mm incl. sample holder |
Weight | 200 g (incl. holder) |
Please avoid introduction of your samples via chamber door as much as possible! |
---|
Installed utility devices
Plasma cleaner (mounted on the chamber) |
Cryo cleaner (mounted on the chamber) |
Fully motorized loadlock |
Analytical detectors specifications
Detector | Parameter | Specified value |
---|
EDS | Detector type | EDAX SDD Octane Super |
---|
Detector chip area | 60 mm2 |
Energy resolution-specified | 129 eV @ MnKα |
Energy resolution-measured | 131.2 eV @ MnKα |
|
EBSD | Detector type | EDAX DigiView IV |
---|
Detector camera resolution | 1392 (H) x 1040 (V) x 12 bits |
Selectable Binning Modes | 1×1 |
1×2 |
2×2 |
4×4 |
8×8 |
10×10 |
Signal / Noise Ratio | > 65 dB |
Data collection rate | up to 150 indexed pps |
|
WDS | Detector type | EDAX TEXS HP XM 4 |
---|
Installed crystals |
---|
Crystal type | Interplanar distance 2d [nm] |
---|
PV7000/38 | 4.01 |
PV7000/33 | 75.47 |
PV7000/35 | 60.491 |
PV7000/43 | 29.769 |
PV7000/36 | 8.721 |
Energy resolution |
---|
Element / line | Resolution – specified [eV] |
---|
C / Kα | 13 |
N / Kα | 18 |
O / Kα | 17 |
Cu / Lα | 30 |
Al / Kα | 28 |
Si / Kα | 6 |
Cu / Kα | 75 |